====== DIY electron microscope ====== {{template>:project:infobox| name=Brmsem| image=:sem.jpg?200| sw=-| hw=-| founder=[[user:mrkva]]| interested= status=active }} ~~META: status = active &relation firstimage = :project:sem.jpg ~~ ===== Overview ===== Goal of this project is to assess whether is possible to build a scanning electron microscope in DIY conditions. There are various sensors that can be used together with SEM - the easiest one to get running is probably the secondary emission detector. However it would be great if we would be able to use backscatter detectors or even X-ray detector for EDX spectroscopy one day! It will also be necessary to get some kind of metal sputtering working to be able to view non-metallic samples. ===== Bill of materials ===== (We'll begin with coarse building blocks and discuss details later) * Vacuum chamber (we have one, check if it is usable) * Base for vacuum chamber with airtight connectors for high and low voltage leads * Vacuum pumps system for fine vacuum * Various power supplies (accelerating voltage, focusing voltage, heater), exact parameters will have to be calculated * electron gun: electron source, electron optics * detector (scintillator + photomultiplier) * display - for initial tests two channel analog oscilloscope with XY mode and z input should be enough (mrkva can provide one). Later, ADC and digital processing is desirable ===== Proposed roadmap ===== * Build and test vacuum pump system to see if we can achieve low enough vacuum (something in the range of 10^-6 Pa will be necessary) * FIXME ===== Useful sources ===== [[http://www.geo.umass.edu/probe/electron%20optics%20-%20lenses.ppt]] [[http://www.reu.pdx.edu/SEM%20Short%20Course.pdf]]